Experiment Number 2

 

 

Use of Density to Determine an Unknown

 

 

 

 

Introduction

 

Purpose:

 

The purpose of this activity is designed to familiarize the student with the use of a balance in the determination of the density of an object and to discuss experimental data in terms of precision and accuracy.  The student will also  become familiar with the use of chemical reference materials.

 

Hypothesis:

 

Based upon your initial observations regarding the various metals, formulate a hypothesis regarding the type of metal (each of these metals is an element).  Remember that a hypothesis should be a deduction based upon observation, i.e. examine the metal and on the basis of what you see or feel record what you think the metal is.  But, be sure to include your justifications, a hypothesis is not just a guess.

 

 

 

 

Materials & Methods

 

Materials:                      Various metals                          Thread

           

Equipment:                   Balance                                    Beaker, 250 mL

           

 

Procedure

 

1.         Together with your group develop a procedure for determining the density of the materials provided.  Your procedure must determine the density of a substance to two significant figures after the decimal place.  Keep in mind our discussion of significant figures with respect to graduated cylinders. 

2.         Using the procedure you have developed, determine the density of the unknowns. You will be provided with a list of the potential unknowns.  Make at least three trials for every metal (why do we do this?).

3.         Use the reference books provided (Merck Index, Lange Handbook of Chemistry or the CRC Handbook of Chemistry and Physics) to determine the identity of the substance.  You can also use various on-line sources.

4.         Construct a data table.  Table should include the unknown letter, mass, mass in water, difference and density.  Data should include three difference pieces of the same metal and two different metals.  Average the density of the two different metals.  Honors:  calculate the standard deviation

5.         In your lab report remember to discuss your results in terms of accuracy and precision, possible sources of error and potential improvements that could be made to the procedure.

 

 

 

 

Questions

 

1.         Why is the density of water 1.0 g/cm3?

2.         What factors other than mass and volume might affect a density determination?

3.         How might density be used to determine the purity of a mixture of gold and silver?

4.         Two spherical objects have the same mass.  One floats in water; the other sinks. Which object has the greater diameter.  Explain your answer.

5.         Mercury is unusual as a metal because it is a liquid a room temperature.  Would gold sink or float in mercury?  Explain your answer.

6.         Density is usually determined at 20º C.  Describe how temperature may affect a density determination.

7.         What is the difference between specific gravity (look up) and density?

8.         An empty beaker weighs 32.4257 g.  A 10-mL pipette sample of an unknown liquid is transferred to the beaker.  The beaker weighs 40.1825 when weighed with the liquid in it.  Calculate the density of the unknown liquid.

9.                   A cylinder has a height of 34 mm and a diameter of 12 mm.  The cylinder weighs 35.65 g.  What is its density?

10.        A sphere has a diameter of 3.25 cm and a mass of 134.2 g.  What is its density?